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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 588027생성일: 2026년 10월 26일

4-[2-(4-Nitro-phenyl)-vinyl]-pyridine → 4-[2-(Pyridin-4-yl)ethyl]aniline

https://huagongshe.com/reaction/588027

반응식

참여 물질

역할이름HCID투입량
반응물4-[2-(4-Nitro-phenyl)-vinyl]-pyridineHCID 307136—
반응물HCID 178418361HCID 178418361—
촉매PalladiumHCID 23938—
용매Ethyl AcetateHCID 8857—
생성물4-[2-(Pyridin-4-yl)ethyl]anilineHCID 233288100%

반응 단계

To the EtOAc solution (30 mL) of 4-[2-(4-nitro-phenyl)-vinyl]-pyridine (160 mg, 0.71 mmol) was added palladium on carbon (0.1 g, 50% wet). The suspension was hydrogenated at 50 psi of hydrogen for 2 hours. The mixture was filtered over a celite pad. The filtrate was concentrate to give 4-(2-pyridin-4-yl-ethyl)-phenylamine as a yellow solid (140 mg, 100%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09227954B2
출처 데이터셋uspto-grants-2016_01
ORD IDord-fbf0b7d100a3482ead33531dc2780fe1
출처 메모uspto-grants-2016_01