Morpholine → HCID 178513121, 화합물
반응식
I.[NH:2]([C:4](SC)=[NH:5])[NH2:3].[NH:8]1[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1>CO>[N:8]1([C:4](=[NH:5])[NH:2][NH2:3])[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1참가 물질
4
실험 절차
To a solution of methyl hydrazinecarbimidothioate hydroiodide (0.100 g, 0.429 mmol) in MeOH (2 mL) was added morpholine (0.075 mL, 0.858 mmol) and refluxed overnight. Reaction was cool to RT and concentrated to get morpholine-4-carboximidhydrazide as a white solid in quantitative yield.
후처리
- temperaturerefluxed overnight
- customReaction
- concentrationconcentrated
출처 및 근거
- ORD 기록
- ord-6407090cb11347459dd3c8c7f1ae4f0f
- 출처 데이터셋
- uspto-grants-2016_01
- 특허 번호
- US09227971B2
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