Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride → HCID 178432000, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride | HCID 2774586 | — |
| 반응물 | HCID 178507542 | HCID 178507542 | — |
| 생성물 | HCID 178432000 | HCID 178432000 | 36% |
반응 단계
The product was prepared according to General Procedure 1, described in Example 1, starting from 5-fluoro-3-methylbenzothiophene-2-sulfonyl chloride (Intermediate 14) (26 mg, 0.10 mmol) and 5-(3-amino-phenyl)tetrazole (31 mg, 0.19 mmol). The title compound was obtained in 36% yield (13.9 mg). MS (ESI+) calcd for C16H12FN5O2S2 389.041644, found 389.042334.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09233946B2 |
| 출처 데이터셋 | uspto-grants-2016_01 |
| ORD ID | ord-e81738f6c1474d4689b642b53cd9f48a |
| 출처 메모 | uspto-grants-2016_01 |