2,4,5-Trichlorobenzenesulfonyl chloride → HCID 178527509, 화합물

HRID 589740

반응식

HRID 589740 반응식
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[C:5]([Cl:9])=[CH:4][C:3]=1[S:10](Cl)(=[O:12])=[O:11].[NH2:14][C:15]1[CH:16]=[C:17]([C:21]2[NH:25][N:24]=[N:23][N:22]=2)[CH:18]=[CH:19][CH:20]=1>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[C:5]([Cl:9])=[CH:4][C:3]=1[S:10]([NH:14][C:15]1[CH:20]=[CH:19][CH:18]=[C:17]([C:21]2[NH:25][N:24]=[N:23][N:22]=2)[CH:16]=1)(=[O:12])=[O:11]

참가 물질

3

반응물 2

HCID 275752,4,5-Trichlorobenzenesulfonyl chlorideHCID 178507542HCID 178507542, 화합물

생성물 1

HCID 178527509HCID 178527509, 화합물수율 57%

실험 절차

The product was prepared according to General Procedure 6, described in Example 65, with 2,4,5-trichlorobenzenesulfonyl chloride (15.4 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 57% yield (11.4 mg). MS (ESI+) calcd mass for C13H8Cl3N5O2S 402.946428, found 402.946388.

후처리

  1. customThe product was prepared

출처 및 근거

ORD 기록
ord-3ce9140ace074024abd18ac5a8aed482
출처 데이터셋
uspto-grants-2016_01
특허 번호
US09233946B2

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