Sulfamide → HCID 86706430, 화합물

HRID 589957노트

반응식

HRID 589957 반응식
[S:1]([NH2:5])([NH2:4])(=[O:3])=[O:2].[O:6]=[S:7]1(=[O:14])[CH2:11][CH2:10][CH:9]([CH2:12]N)[CH2:8]1>O>[O:6]=[S:7]1(=[O:14])[CH2:11][CH2:10][CH:9]([CH2:12][NH:4][S:1](=[O:3])(=[O:2])[NH2:5])[CH2:8]1

참가 물질

4

반응물 2

HCID 82267SulfamideHCID 27722253-(Aminomethyl)-1lambda~6~-thiolane-1,1-dione

생성물 1

HCID 86706430HCID 86706430, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Sulfamide (2.4 mmol) was dissolved in H2O (10 mL), added (1,1-dioxothiolan-3-yl)methanamine (2 mmol) and stirred at reflux for 16 h. The obtained reaction mixture was cooled to rt and freezedried affording the title compound as an oil. Used without further purification.

후처리

  1. temperatureat reflux for 16 h
  2. customThe obtained reaction mixture
  3. customfreezedried

출처 및 근거

ORD 기록
ord-bc55470bd0764475824846dcf93f7959
출처 데이터셋
uspto-grants-2016_01
특허 번호
US09233964B2

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