Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → HCID 178463316, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Orcinol | HCID 10436 | — |
| 반응물 | Ammonium Persulfate | HCID 62648 | — |
| 반응물 | N-Ethyl-N-isopropyl-p-phenylenediamine hydrochloride | HCID 16211123 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178463316 | HCID 178463316 | — |
반응 단계
To a solution of 0.002 mol (429 mg) of N-ethyl-N-isopropyl-4-aminoaniline hydrochloride and 0.001 mol (124 mg) of orcinol in 2 ml of water and 6 ml of ethanol brought to a pH of 9.5 with a solution of 20% aqueous ammonia, 0.002 mol (456 mg) of ammonium persulfate dissolved in 1 ml of water is added dropwise. The temperature is held below 30° C. during the addition. At the end of the addition, the precipitate formed is filtered and washed with water.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09439844B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-4cf052ea8c254f09bf3992e6e71354c9 |
| 출처 메모 | uspto-grants-2016_09 |