Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl bromide → Diethyl allylphosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl bromide | HCID 7841 | — |
| 반응물 | Triethyl phosphite | HCID 31215 | — |
| 생성물 | Diethyl allylphosphonate | HCID 573014 | — |
반응 단계
Allyl bromide was treated with triethylphosphite in the absence of solvent using microwave conditions at 150° C. to give diethyl allylphosphonate. Diethyl allylphosphonate was combined with bromotrimethyl silane and subsequently quenched with methanol to afford diethyl allylphosphonic acid according to Scheme 7.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09234985B2 |
| 출처 데이터셋 | uspto-grants-2016_01 |
| ORD ID | ord-0e82b32ecb924645bc132c8becf71036 |
| 출처 메모 | uspto-grants-2016_01 |