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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 590895생성일: 2026년 10월 25일

Ethanol → Sodium 1,3,5-tricyclohexylbenzenesulfonate

https://huagongshe.com/reaction/590895

반응식

참여 물질

역할이름HCID투입량
반응물EthanolHCID 702—
반응물Sodium HydroxideHCID 14798—
반응물Chlorosulfonic acidHCID 24638—
반응물TricyclohexylbenzeneHCID 3015433—
용매DichloromethaneHCID 6344—
생성물Sodium 1,3,5-tricyclohexylbenzenesulfonateHCID 86655172—

반응 조건

온도3 °C

반응 단계

Tricyclohexylbenzene amounting to 30 g was dissolved in 50 ml of methylene chloride and agitated while cooling at 3° C. Then, 15.2 g of chlorosulfonic acid was slowly dropped into the solution. After the completion of the dropping, the mixture was agitated at room temperature for five hours. Subsequently, 10 g of ice and then 40 g of 50% aqueous sodium hydroxide solution was poured into the mixture. Further, 20 g of ethanol was added and agitated at 50° C. for an hour. Any insoluble matter was removed by filtration, and the product was subjected to vacuum distillation at 40° C. The thus obtained crystal was collected by filtration, and washed with hexane, thereby obtaining 30 g of sodium 1,3,5-tricyclohexylbenzenesulfonate.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09235116B2
출처 데이터셋uspto-grants-2016_01
ORD IDord-43f04fccdfa146fda9f1cee1f1fec542
출처 메모uspto-grants-2016_01