Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorobutanol → Methacrylic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorobutanol | HCID 5977 | — |
| 반응물 | Methyl 2-chloro-2-methylpropanoate | HCID 211144 | — |
| 생성물 | Methacrylic Acid | HCID 4093 | — |
| 생성물 | Methyl Methacrylate | HCID 6658 | — |
| 생성물 | (1,1,1-Trichloro-2-methyl-2-propyl) methacrylate | HCID 118163057 | — |
| 생성물 | (1,1,1-Trichloro-2-methyl-2-propyl) 2-chloro-2-methylpropanoate | HCID 118163068 | — |
반응 단계
The analysis of the crude reaction solution by gas chromatography revealed that the conversion of 1,1,1-trichloro-2-methyl-2-propanol was 70.0% and the yield of methyl 2-chloro-2-methylpropanoate was 23.9%. As to other products, it was obtained methyl methacrylate in a 0.7% yield, methacrylic acid in a 0.2% yield, (1,1,1-trichloro-2-methyl-2-propyl) methacrylate in a 7.8% yield, and (1,1,1-trichloro-2-methyl-2-propyl) 2-chloro-2-methylpropanoate in a 12.9% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09238612B2 |
| 출처 데이터셋 | uspto-grants-2016_01 |
| ORD ID | ord-cd5ea02083ee44c7be71b659732e9e78 |
| 출처 메모 | uspto-grants-2016_01 |