참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Benzoic Acid | HCID 243 | — |
| 반응물 | Benzoselenazolinone | HCID 87879929 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 6-Benzoylbenzoselenazolinone | HCID 131718172 | — |
반응 단계
1.98 g (0.01 mol) of benzoselenazolinone, 50 to 60 g of polyphosphoric acid and 1.35 g (0.011 mol) of benzoic acid are introduced into a 100-cm3 round-bottomed flask. The mixture is heated on an oil bath to a temperature of 130° C. for a time T of 3 hours, with stirring. The reaction mixture is then hydrolyzed in 300 cm3 of cold water. The product is drained, washed with water, dried and recrystallized.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05246951 |
|---|
| 출처 데이터셋 | uspto-grants-1993_09 |
|---|
| ORD ID | ord-cac88bd35cc64efb905597bc14f2064b |
|---|
| 출처 메모 | uspto-grants-1993_09 |
|---|
