Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalyl chloride → 2-Chloro-6-methylbenzoyl isocyanate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | Benzamide, 2-chloro-6-methyl- | HCID 113589 | — |
| 용매 | 1,2-Dichloroethane | HCID 11 | — |
| 생성물 | 2-Chloro-6-methylbenzoyl isocyanate | HCID 90019597 | 86.7% |
반응 단계
The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 2-chloro-6-methylbenzamide (1.0 g, 5.9 mmol), oxalyl chloride (0.894 g, 7.1 mmol) and EDC (20 mL) to afford 1.00 g of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09439890B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-1eea1c649c4e4c389264d24d65d8cc40 |
| 출처 메모 | uspto-grants-2016_09 |