2-Bromopyridine → 2-Nitro-4-(2-pyridinyl)benzaldehyde

HRID 593452노트

반응식

HRID 593452 반응식
[N+:1]([C:4]1[CH:11]=[C:10](B2OC(C)(C)C(C)(C)O2)[CH:9]=[CH:8][C:5]=1[CH:6]=[O:7])([O-:3])=[O:2].Br[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][N:23]=1>O1CCOCC1>[N+:1]([C:4]1[CH:11]=[C:10]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][N:23]=2)[CH:9]=[CH:8][C:5]=1[CH:6]=[O:7])([O-:3])=[O:2]

참가 물질

4

반응물 2

HCID 79732-BromopyridineHCID 754875122-Nitro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde

생성물 1

HCID 866534802-Nitro-4-(2-pyridinyl)benzaldehyde

시약·촉매·용매 1

HCID 312751,4-Dioxane용매

실험 절차

The title compound was prepared by the procedure as described in Example 101 (Step C) using 2-nitro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde and 2-bromopyridine in dioxane (reflux).

출처 및 근거

ORD 기록
ord-807e4c183e4b45a689b76ea445f0bba1
출처 데이터셋
uspto-grants-2016_01
특허 번호
US09242964B2

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