Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalyl chloride → 4-Chloro-2-fluorobenzoyl isocyanate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 4-Chloro-2-fluorobenzamide | HCID 3721849 | — |
| 용매 | 1,2-Dichloroethane | HCID 11 | — |
| 생성물 | 4-Chloro-2-fluorobenzoyl isocyanate | HCID 54541725 | — |
반응 단계
The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 4-chloro-2-fluorobenzamide (0.200 g, 1.26 mmol), EDC (10 mL) and oxalyl chloride (0.14 mL, 1.15 mmol) to afford 0.200 g of the product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09439890B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-095f2e6e126d43ed8bd093d566c00aba |
| 출처 메모 | uspto-grants-2016_09 |