Oxalyl chloride → 4-(Bromomethyl)benzoyl isocyanate
반응식
[Br:1][CH2:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([NH2:9])=[O:8])=[CH:5][CH:4]=1.C(Cl)(=O)[C:13](Cl)=[O:14]>C(Cl)CCl>[Br:1][CH2:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([N:9]=[C:13]=[O:14])=[O:8])=[CH:5][CH:4]=1참가 물질
4
실험 절차
The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 4-(bromomethyl)benzamide (0.200 g), oxalyl chloride (0.012 mL) and EDC (15 mL) to afford 0.150 g of the desired product.
후처리
- customThe title compound was prepared
출처 및 근거
- ORD 기록
- ord-407fd253c6b44db9b13486776b9d965c
- 출처 데이터셋
- uspto-grants-2016_09
- 특허 번호
- US09439890B2
반응 노트
불러오는 중…