Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dibenzo(b,d)furan-2-carboxaldehyde → 1-(Dibenzo[b,d]furan-2-ylmethyl)-7-(2,6-dimethoxyphenyl)azepan-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dibenzo(b,d)furan-2-carboxaldehyde | HCID 220843 | — |
| 반응물 | Methyl 6-amino-6-(2,6-dimethoxyphenyl)hexanoate | HCID 69082587 | — |
| 생성물 | 1-(Dibenzo[b,d]furan-2-ylmethyl)-7-(2,6-dimethoxyphenyl)azepan-2-one | HCID 69081081 | — |
반응 단계
Prepared according to the described general procedure 1 (GP1) by reaction of methyl 6-amino-6-(2,6-dimethoxyphenyl)hexanoate with commercially available dibenzo[b,d]furan-2-carbaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions I): tR=1.53 min.; [M+H]+: 430.13 g/mol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09242970B2 |
| 출처 데이터셋 | uspto-grants-2016_01 |
| ORD ID | ord-98d301aeeff34de6beddf4b397abe0b0 |
| 출처 메모 | uspto-grants-2016_01 |