Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → Ethyl 4-chlorobutyrate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | 4-Chlorobutanoic acid | HCID 12300 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | Ethyl 4-chlorobutyrate | HCID 18474 | — |
반응 단계
SOCl2 (60.0 mL, 820 mmol) was added to a solution of 4-chloro-butyric acid (50.0 g, 410 mmol) in EtOH (1.2 L) at 0° C. The mixture was heated to reflux for 2 hr then cooled to room temperature and concentrated under reduced pressure to afford the crude 4-chloro-butyric acid ethyl ester.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09242984B2 |
| 출처 데이터셋 | uspto-grants-2016_01 |
| ORD ID | ord-917bd02f027c47efa868f43de331fd4b |
| 출처 메모 | uspto-grants-2016_01 |