Isoprene → Isoprene acrylonitrile

HRID 595620

반응식

HRID 595620 반응식
[CH2:1]=[CH:2][C:3](=[CH2:5])[CH3:4].[C:6](#[N:9])[CH:7]=[CH2:8]>>[CH2:1]=[CH:2][C:3](=[CH2:4])[CH3:5].[C:6](#[N:9])[CH:7]=[CH2:8]

참가 물질

3

실험 절차

Then, were added thereto 68.2 parts of isoprene and 1.79 parts of 2-chloropropionitrile as an organic halide, and stirred under heating at 80° C. to conduct a polymerization reaction. After 114 hours, the glass reaction vessel was cooled in a dry ice-methanol bath, and the volatiles were distilled off under reduced pressure to give a random (isoprene/acrylonitrile) copolymer. The conversion rate of isoprene was 84% and the conversion rate of acrylonitrile was 76%. The analysis results of the random (isoprene/acrylonitrile) polymer obtained are shown in Table 5. The polymer was confirmed to have a chlorine atom at the terminal of the polymer chain.

출처 및 근거

ORD 기록
ord-b420f60afc9f41019e26bed48f0ac137
출처 데이터셋
uspto-grants-2016_01
특허 번호
US09243100B2

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