Bromomethyl 4-methoxyphenyl ketone → N-(4-chlorophenacyl) pyridazinium chloride

HRID 596723

반응식

HRID 596723 반응식
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][N:2]=1.COC1C=CC(C(=O)CBr)=CC=1.[Cl:19][C:20]1[CH:29]=[CH:28][C:23]([C:24](=[O:27])[CH2:25]Cl)=[CH:22][CH:21]=1>N1C=CC=CC=1>[Cl-:19].[Cl:19][C:20]1[CH:29]=[CH:28][C:23]([C:24](=[O:27])[CH2:25][N+:1]2[CH:6]=[CH:5][CH:4]=[CH:3][N:2]=2)=[CH:22][CH:21]=1

참가 물질

5

반응물 3

HCID 4965Bromomethyl 4-methoxyphenyl ketoneHCID 9259PyridazineHCID 702982,4'-Dichloroacetophenone

생성물 1

HCID 86734540N-(4-chlorophenacyl) pyridazinium chloride

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

Employing the procedure of Example I but replacing pyridine with a substantially equimolecular amount of pyridazine and replacing 4-methoxyphenacyl bromide with a substantially equimolecular amount of 4-chlorophenacyl chloride there is obtained N-(4-chlorophenacyl) pyridazinium chloride, a solid soluble in water.

출처 및 근거

ORD 기록
ord-6e87b6dd681d4db6920a8772c4d5d4ea
출처 데이터셋
uspto-grants-1977_03
특허 번호
USRE029153

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