Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → N-(1,3-dioxolan-5-ylmethyl)-2,6-dimethyl-4-bromoaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 4-Bromo-2,6-xylidine | HCID 90549 | — |
| 반응물 | 4-(Chloromethyl)-1,3-dioxolane | HCID 240153 | — |
| 촉매 | Tetraethylammonium Chloride | HCID 5946 | — |
| 생성물 | N-(1,3-dioxolan-5-ylmethyl)-2,6-dimethyl-4-bromoaniline | HCID 21447802 | — |
반응 단계
2,6-Dimethyl-4-bromoaniline (0.3 mole), 5-chloromethyl-1,3-dioxolane (0.3 mole), potassium carbonate (0.3 mole) and tetraethylammonium chloride (2 grams) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux for a period of 5 hours. After this time the mixture is filtered and distilled to yield the desired product N-(1,3-dioxolan-5-ylmethyl)-2,6-dimethyl-4-bromoaniline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04012222 |
| 출처 데이터셋 | uspto-grants-1977_03 |
| ORD ID | ord-7817933fbf3f446c876e88053d9ca1f2 |
| 출처 메모 | uspto-grants-1977_03 |