Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propylamine → 2-methyl-N-propylalaninamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propylamine | HCID 7852 | — |
| 반응물 | Methyl 2-amino-2-methylpropanoate | HCID 4186341 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-methyl-N-propylalaninamide | HCID 21448036 | — |
반응 단계
To a solution of 26.3 parts of methyl 2-amino-2-methylpropionate in methanol is added 70 parts of n-propylamine. The mixture is placed in a bomb and left at a temperature of 100° C. for one week. The solvents are then stripped off under reduced pressure. Distillation of the residual oil affords N1 -propyl-2-amino-2-methylpropionamide, boiling at 58° C. at 0.1 mm pressure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04012367 |
| 출처 데이터셋 | uspto-grants-1977_03 |
| ORD ID | ord-065463928e104051adfab8401ac48500 |
| 출처 메모 | uspto-grants-1977_03 |