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Diethylaminoethyl chloride → 1-(3',4',5'-Trimethoxy benzyl)-2-phenyl-4-diethylamino ethyl piperazine

HRID 596863
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반응식

HRID 596863 반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:19]=[C:20]([O:24][CH3:25])[C:21]=1[O:22][CH3:23])[CH2:6][N:7]1[CH2:12][CH2:11][NH:10][CH2:9][CH:8]1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.[CH2:26]([N:28]([CH2:31][CH2:32]Cl)[CH2:29][CH3:30])[CH3:27]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:19]=[C:20]([O:24][CH3:25])[C:21]=1[O:22][CH3:23])[CH2:6][N:7]1[CH2:12][CH2:11][N:10]([CH2:27][CH2:26][N:28]([CH2:31][CH3:32])[CH2:29][CH3:30])[CH2:9][CH:8]1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

3

반응물 2

HCID 13364Diethylaminoethyl chlorideHCID 214485551-(3',4',5'-Trimethoxy benzyl)-2-phenyl piperazine

생성물 1

HCID 867330251-(3',4',5'-Trimethoxy benzyl)-2-phenyl-4-diethylamino ethyl piperazine

실험 절차

1-(3',4',5'-Trimethoxy benzyl)-2-phenyl piperazine prepared according to Example 11, is alkylated by means of diethylamino ethylchloride by following the procedure described in Example 2 (c). The resulting reaction product is obtained in the form of yellow oil boiling at 200° C./0.03 mm. Hg.

후처리

  1. customThe resulting reaction product

출처 및 근거

ORD 기록
ord-6656cb39b37048388957ee899cdbd2ee
출처 데이터셋
uspto-grants-1977_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04012389

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