Borane → 1H-1,4-Benzodiazepine

HRID 597076

반응식

HRID 597076 반응식
[N:1]1(CC(N)=O)[C:7]2[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=2[CH:5]=[N:4][CH:3]=[CH:2]1.B>>[NH:1]1[C:7]2[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=2[CH:5]=[N:4][CH:3]=[CH:2]1

참가 물질

3

반응물 2

HCID 6331BoraneHCID 23201858HCID 23201858, 화합물

생성물 1

HCID 1484311H-1,4-Benzodiazepine

실험 절차

In the manner given in Example 1, N,N-dimethyl-8-chloro-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4benzodiazepine-1-acetamide is reduced with borane to give 1-[2-(dimethylamino)ethyl]-8-chloro-5,6-dihydro-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4-benzodiazepine.

출처 및 근거

ORD 기록
ord-e0395511b599499fbaf3969958104e68
출처 데이터셋
uspto-grants-1977_03
특허 번호
US04012413

연결된 노트

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