Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Borane → 1H-1,4-Benzodiazepine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Borane | HCID 6331 | — |
| 반응물 | N,N-diethyl-4-methyl-8-fluoro-6-(o-fluorophenyl)-4H-s-triazolo[4,3-a]-[1,4]benzodiazepine-1-acetamide | HCID 21449044 | — |
| 생성물 | 1H-1,4-Benzodiazepine | HCID 148431 | — |
반응 단계
In the manner given in Example 1, N,N-diethyl-4-methyl-8-fluoro-6-(o-fluorophenyl)-4H-s-triazolo[4,3-a]-[1,4]benzodiazepine-1-acetamide is reduced with borane to give 1-[2-diethylamino)ethyl]-4-methyl-8-fluoro-5,6-dihydro-6-(o-fluorophenyl)-4H-s-triazolo]4,3-a][1,4]benzodiazepine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04012413 |
| 출처 데이터셋 | uspto-grants-1977_03 |
| ORD ID | ord-f28aa78997034200b083d17358eb3950 |
| 출처 메모 | uspto-grants-1977_03 |