참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Thiocarbohydrazide | HCID 2724189 | — |
| 반응물 | 2,2-Dibromo-3,3-dimethylbutyric acid | HCID 21446894 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178441961 | HCID 178441961 | — |
반응 단계
A mixture of 2,2-dibromo-3,3-dimethylbutyric acid, 55 parts, and thiocarbohydrazide, 22 parts, in 500 parts of (1:1) methanol and water was heated to reflux for five hours. Upon cooling the reaction mixture to 0° C., a solid formed and was collected. The solid, 4-amino-6-t-butyl-3-mercapto-1,2,4-triazin-5-one, was obtained in 78% of theory (29 parts).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04013649 |
|---|
| 출처 데이터셋 | uspto-grants-1977_03 |
|---|
| ORD ID | ord-e22668be1d1948199e90abab48666f87 |
|---|
| 출처 메모 | uspto-grants-1977_03 |
|---|
