1-Iodopropane → 4(1H)-Pyridazinone, 3,5-diphenyl-1-propyl-

반응식

[CH2:1](I)[CH2:2][CH3:3].[C:5]1([C:11]2[C:16](=[O:17])[C:15]([C:18]3[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=3)=[CH:14][NH:13][N:12]=2)[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1>>[C:5]1([C:11]2[C:16](=[O:17])[C:15]([C:18]3[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=3)=[CH:14][N:13]([CH2:1][CH2:2][CH3:3])[N:12]=2)[CH:6]=[CH:7][CH:8]=[CH:9][CH:10]=1

참가 물질

반응물 2

HCID 336431-Iodopropane

HCID 6192033,5-Diphenyl-1H-pyridazin-4-one

생성물 1

HCID 122629924(1H)-Pyridazinone, 3,5-diphenyl-1-propyl-수율 95%

실험 절차

Propyl iodide was reacted with 3,5-diphenyl-4(1H)-pyridazinone according to the process of Example 4 to produce 3,5-diphenyl-1-propyl-4(1H)-pyridazinone, m.p. 94°-96° C. in 95% yield.

출처 및 근거

ORD 기록: ord-0cf446f0cba148ff9eac7f15468e9f02
출처 데이터셋: uspto-grants-1977_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04013658

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