Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 178503824, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Cysteamine Hydrochloride | HCID 9082 | — |
| 반응물 | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| 반응물 | Picrate | HCID 4432340 | — |
| 반응물 | HCID 178479151 | HCID 178479151 | — |
| 반응물 | HCID 178511470 | HCID 178511470 | — |
| 생성물 | HCID 178503824 | HCID 178503824 | — |
반응 단계
Reaction of 2-amino-4-hydroxymethylimidazole hydrochloride (which is obtained by treating the picrate salt with hydrochloric acid) with cysteamine hydrochloride and reaction of the resulting 2-amino-4-[(2-aminoethyl)-thiomethyl]imidazole with 1-nitro-2,2-bis-methylthioethylene according to the procedure of Example 8(i) gives 1-nitro-2-methylthio-2-[2-((2-amino-4-imidazolyl)methylthio)-ethylamino]ethylene. Finally, reaction with 2-[(2-aminoethyl)thiomethyl]-3-chloropyridine by the procedure of Example 1 (a)(ii) produces the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04013769 |
| 출처 데이터셋 | uspto-grants-1977_03 |
| ORD ID | ord-b1c6cfb86095455ab6118d489d5799bb |
| 출처 메모 | uspto-grants-1977_03 |