Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzenemethanamine, 3,4-dichloro- → 4-((3,4-Dichlorobenzyl)amino)benzo[d][1,2,3]triazine-8-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzenemethanamine, 3,4-dichloro- | HCID 1608 | — |
| 반응물 | 4-oxo-1H-1,2,3-benzotriazine-8-carboxamide | HCID 178513613 | — |
| 생성물 | 4-((3,4-Dichlorobenzyl)amino)benzo[d][1,2,3]triazine-8-carboxamide | HCID 74538689 | — |
반응 단계
Compound 2 was prepared following general synthetic scheme 7 wherein (3,4-dichlorophenyl)methanamine was reacted with 4-hydroxybenzo[d][1,2,3]-triazine-8-carboxamide to give the title compound. LC-MS [350 (M+1)], 1H NMR (400 MHz, DMSO-d6): δ 9.37 (s, 1H), 9.31 (t, 1H), 8.54 (d, 1H), 8.49 (d, 1H), 8.05 (s, 1H), 8.00 (t, 1H), 7.70 (s, 1H), 7.60 (d, 1H), 7.40 (d, 1H), 4.90 (d, 1H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09440968B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-03bfa14da0a648559a9d736cfbfbcce9 |
| 출처 메모 | uspto-grants-2016_09 |