Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Tert-butyl-2-nitrobenzoic acid → 2-Amino-4-tert-butylbenzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Tert-butyl-2-nitrobenzoic acid | HCID 257326 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Amino-4-tert-butylbenzoic acid | HCID 14645872 | 10.3% |
반응 단계
4-tert-Butyl-2-nitro-benzoic acid (199 mg, 8.91 mmol), and 10% palladium on carbon (40 mg) were stirred in 6 mL ethanol under an atmosphere of hydrogen for 3 hours. The resulting mixture was filtered and concentrated in vacuo to yield 2-Amino-4-tert-butyl-benzoic acid (177 mg, 0.916 mmol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07902194B2 |
| 출처 데이터셋 | uspto-grants-2011_03 |
| ORD ID | ord-e422b9e77b964f47ae300cabc0da87c4 |
| 출처 메모 | uspto-grants-2011_03 |