Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → N-Amylurea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Pentane, 1-isocyanato- | HCID 206036 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | N-Amylurea | HCID 198194 | — |
반응 단계
To a 7.0 M solution of ammonia in methanol (32 mL) was dropwise added 1-isocyanatopentane (5.0 g, 0.044 mol). After the addition, the mixture was stirred at room temperature for 1 h and concentrated under reduced pressure to give a white solid, which was directly used for next step without further purification. LCMS calculated for C6H15N2O (M+H): 131.1. found 131.1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07902205B2 |
| 출처 데이터셋 | uspto-grants-2011_03 |
| ORD ID | ord-23d6f2bf577e4920b65514a6eac45681 |
| 출처 메모 | uspto-grants-2011_03 |