Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 53416493, 화합물 → HCID 67228763, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 53416493 | HCID 53416493 | — |
| 반응물 | 2-Ethoxy-8-isothiocyanato-1,4-dihydronaphthalene | HCID 86609612 | — |
| 반응물 | HCID 86609614 | HCID 86609614 | — |
| 반응물 | HCID 86609615 | HCID 86609615 | — |
| 생성물 | HCID 67228763 | HCID 67228763 | 16% |
반응 단계
The title compound was prepared using the procedure as described in Example 1H, substituting the product of Example 20F (415 mg, 1.36 mmol) for the product of Example 1F and the product of Example 22A (404 mg, 1.63 mmol) for the product of Example 1G. The crude product was purified by flash chromatography eluting with 20% to 60% EtOAc/hexanes which gave 107 mg (16%) of the title compound as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07902236B2 |
| 출처 데이터셋 | uspto-grants-2011_03 |
| ORD ID | ord-8a3701485d6247e7843411af5deb8e45 |
| 출처 메모 | uspto-grants-2011_03 |