Pentafluoroaniline → 501670-16-2

HRID 601095

반응식

HRID 601095 반응식
[C:1]([C:5]1[CH:10]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[CH:8]=[C:7]([CH:15]=NC2C(Br)=CC=CC=2Br)[C:6]=1[OH:25])([CH3:4])([CH3:3])[CH3:2].[F:26][C:27]1[C:33]([F:34])=[C:32]([F:35])[C:31]([F:36])=[C:30]([F:37])[C:28]=1[NH2:29].C(C1C(O)=C(C=C(C(C)(C)C)C=1)C=O)(C)(C)C>>[C:1]([C:5]1[CH:10]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[CH:8]=[C:7]([CH:15]=[N:29][C:28]2[C:27]([F:26])=[C:33]([F:34])[C:32]([F:35])=[C:31]([F:36])[C:30]=2[F:37])[C:6]=1[OH:25])([CH3:4])([CH3:3])[CH3:2]

참가 물질

4

반응물 3

HCID 13040PentafluoroanilineHCID 6880233,5-Di-tert-butylsalicylaldehydeHCID 136346710HCID 136346710, 화합물

생성물 1

HCID 135509894501670-16-2

실험 절차

Employing an analogous procedure to that described above for the synthesis of 2,4-bis(tert-butyl)-6-[[(2,6-dibromophenyl)imino]methyl]phenol, 2,3,4,5,6-pentafluoroaniline (0.54 g, 2.9 mmol) was added to 3,5-di-tert-butyl-2-hydroxybenzaldehyde (0.70 g, 2.9 mmol). The product was purified by recrystallisation from hot MeOH and isolated as yellow crystals.

후처리

  1. customThe product was purified by recrystallisation from hot MeOH
  2. customisolated as yellow crystals

출처 및 근거

ORD 기록
ord-1224c7f7869c44258aeb252783b2e5e7
출처 데이터셋
uspto-grants-2011_03
특허 번호
US07902308B2

연결된 노트

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