Ethyl 2-aminocyclohex-1-ene-1-carboxylate → 5,6,7,8-tetrahydro-2H-3,1-benzoxazine-2,4(1H)-dione
반응식
[NH2:1][C:2]1[CH2:7][CH2:6][CH2:5][CH2:4][C:3]=1[C:8]([O:10][CH2:11]C)=[O:9].C(C(CC)CNC1N=CC=CC=1C(OCC)=[O:21])C>>[NH:1]1[C:2]2[CH2:7][CH2:6][CH2:5][CH2:4][C:3]=2[C:8](=[O:9])[O:10][C:11]1=[O:21]참가 물질
3
실험 절차
The title compound was prepared according to the procedure of Example 3B substituting ethyl 2-aminocyclohex-1-ene-1-carboxylate for the product of Example 3A (0.960 g, 97%). MS (ESI−) m/z 166 (M−H)+.
출처 및 근거
- ORD 기록
- ord-be9104209980441490f19aced8f83fa6
- 출처 데이터셋
- uspto-grants-2011_03
- 특허 번호
- US07902203B2
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