참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methacrylic Acid | HCID 4093 | — |
| 반응물 | 2-Methyl-4-oxatricyclo[5.2.1.02,6]decan-3-yl acetate | HCID 66930811 | — |
| 촉매 | 2,2'-Methylenebis(4-methyl-6-tert-butylphenol) | HCID 8398 | — |
| 생성물 | 2-Methyl-4-oxatricyclo[5.2.1.02,6]decan-3-yl methacrylate | HCID 66930799 | 91% |
반응 단계
A mixture of 73 g of 2-methyl-4-oxatricyclo[5.2.1.02,6]-decan-3-yl acetate, 150 g of methacrylic acid, and 40 mg of 2,2′-methylenebis(6-t-butyl-p-cresol) was heated at 50° C. under atmospheric pressure for 30 minutes, after which under a reduced pressure of 0.20 kPa, the reaction mixture was heated for 18 hours for distilling off the acetic acid formed. The reaction mixture was purified by distillation, obtaining 72 g (yield 91%) of the target compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07902385B2 |
|---|
| 출처 데이터셋 | uspto-grants-2011_03 |
|---|
| ORD ID | ord-a4e26a2840e440c09d215439599b115c |
|---|
| 출처 메모 | uspto-grants-2011_03 |
|---|
