Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Eugenol → 4-Propylguaiacol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Eugenol | HCID 3314 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | 4-Propylguaiacol | HCID 17739 | — |
반응 단계
Palladium-carbon (5 mass %, 54 mg) was added to a 2-propanol (2.5 mL) solution of eugenol (CAS No. 97-53-0, 500 mg) under an argon atmosphere. The resultant mixture was vigorously stirred at an external temperature of 50° C. under a hydrogen flow for about 4.5 hours. The reaction solution was filtered through Celite, and the filtrate was concentrated, to thereby obtain the title compound (447 mg) having the following physical properties.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07906549B2 |
| 출처 데이터셋 | uspto-grants-2011_03 |
| ORD ID | ord-4e043d5306dd4568b3fe3a8036310df1 |
| 출처 메모 | uspto-grants-2011_03 |