Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Dichlorophenol → N-(2',6'-dichlorophenyl)-N-chloroacetyl-4-methylaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Dichlorophenol | HCID 6899 | — |
| 반응물 | 2-Chloro-N-(4-methylphenyl)acetamide | HCID 27967 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-(2',6'-dichlorophenyl)-N-chloroacetyl-4-methylaniline | HCID 57952147 | — |
반응 단계
Same procedure as example 6a starting from 2,6-dichlorophenol and 2-chloro-N-(4-methylphenyl)acetamide. At the end of the acetylation reaction the mixture was diluted with a small amount of toluene (0.2 part) to prevent solidification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07906677B2 |
| 출처 데이터셋 | uspto-grants-2011_03 |
| ORD ID | ord-af3bd9ab2c584e5988f942de2ef192e8 |
| 출처 메모 | uspto-grants-2011_03 |