Sulfuryl chloride → 2,6-Dimethoxybenzenesulfonyl chloride

반응식

Br[C:2]1[C:7]([O:8][CH3:9])=[CH:6][CH:5]=[CH:4][C:3]=1[O:10][CH3:11].[S:12](Cl)([Cl:15])(=[O:14])=[O:13]>>[CH3:11][O:10][C:3]1[CH:4]=[CH:5][CH:6]=[C:7]([O:8][CH3:9])[C:2]=1[S:12]([Cl:15])(=[O:14])=[O:13]

참가 물질

반응물 2

HCID 24648Sulfuryl chloride

HCID 6122962-Bromo-1,3-dimethoxybenzene

생성물 1

HCID 154110502,6-Dimethoxybenzenesulfonyl chloride

실험 절차

2,6-Dimethoxybenzenesulfonyl chloride was prepared from 2-bromo-1,3-dimethoxybenzene according to the procedure in Example 1, Step 1. The reaction gave a mixture of sulfonyl chloride and another product as a white solid.

후처리

customThe reaction gave

출처 및 근거

ORD 기록: ord-5ef0ad4d861643f1848796d3d60755f5
출처 데이터셋: uspto-grants-2011_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07906548B2

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