Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 605791생성일: 2026년 10월 25일
Triphenylphosphine → Phosphonium, [[3-(methoxycarbonyl)phenyl]methyl]triphenyl-, bromide
https://huagongshe.com/reaction/605791
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 반응물 | Methyl 3-(bromomethyl)benzoate | HCID 517981 | — |
| 생성물 | Phosphonium, [[3-(methoxycarbonyl)phenyl]methyl]triphenyl-, bromide | HCID 10051285 | 100.3% |
반응 단계
Triphenylphosphine (85.8 g) was added to a Tol (400 ml) solution of methyl 3-bromomethylbenzoate (50.0 g), followed by stirring at 80° C. for 10 hours. After this was cooled to room temperature, the crystal precipitated was collected by filtration and washed with Tol. This was dried under reduced pressure to obtain (3-methoxycarbonylbenzyl)(triphenyl)phosphonium bromide (107.6 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US07915261B2 |
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| 출처 데이터셋 | uspto-grants-2011_03 |
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| ORD ID | ord-e78920478d8f44d99091fe0c36185b41 |
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| 출처 메모 | uspto-grants-2011_03 |
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