Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chloro-3-nitrotoluene → 4-Ethyl-2-nitro-1-phenylsulfanyl-benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chloro-3-nitrotoluene | HCID 6976 | — |
| 반응물 | Sodium benzenethiolate | HCID 4110039 | — |
| 반응물 | 1-Chloro-4-ethyl-2-nitro-benzene | HCID 13792156 | — |
| 생성물 | 4-Ethyl-2-nitro-1-phenylsulfanyl-benzene | HCID 57469913 | — |
반응 단계
Sodium thiophenolate was reacted with 1-Chloro-4-ethyl-2-nitro-benzene according to the procedure from Example 5H substituting 1-Chloro-4-ethyl-2-nitro-benzene for 4-chloro-3-nitrotoluene to provide 4-Ethyl-2-nitro-1-phenylsulfanyl-benzene which was reduced according to the procedure from Example 5I to provide the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07915411B2 |
| 출처 데이터셋 | uspto-grants-2011_03 |
| ORD ID | ord-54d11cb98c094a3eb4ceb54b11cb6cc4 |
| 출처 메모 | uspto-grants-2011_03 |