1H-1,2,4-Triazole → 5-methyl-2-(1H-1,2,4-triazol-1-yl)benzoic acid

반응식

[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([N:11]2[N:15]=[CH:14]C=N2)=[C:6]([CH:10]=1)[C:7]([OH:9])=[O:8].[NH:16]1[CH:20]=NC=N1>>[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([N:11]2[CH:20]=[N:16][CH:14]=[N:15]2)=[C:6]([CH:10]=1)[C:7]([OH:9])=[O:8]

참가 물질

반응물 2

HCID 92571H-1,2,4-Triazole

HCID 532601655-methyl-2-(2H-1,2,3-triazol-2-yl)benzoic acid

생성물 1

HCID 625146105-methyl-2-(1H-1,2,4-triazol-1-yl)benzoic acid

실험 절차

The title compound was synthesized following the same general protocol as described for 5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoic acid in Example A11 using 1H-1,2,4-triazole. ESI-MS (m/z): 204 [M+1]+.

출처 및 근거

ORD 기록: ord-3e825d5307b540d1b2e4257af17db1a1
출처 데이터셋: uspto-grants-2016_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09440982B2

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