Ammonia → 4-Chlorophenyl-2-thiourea

HRID 609570노트

반응식

HRID 609570 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]=[C:9]=[S:10])=[CH:4][CH:3]=1.[NH3:11]>CCOCC>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]([NH2:11])=[S:10])=[CH:4][CH:3]=1

참가 물질

4

반응물 2

HCID 222AmmoniaHCID 164804-Chlorophenyl isothiocyanate

생성물 1

HCID 7358434-Chlorophenyl-2-thiourea

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

A stirred solution of 4-chlorophenyl isothiocyanate (10.0 g, 0.077 mol) in 100 ml ether was saturated with ammonia gas for five minutes. The reaction mixture was then stirred for 18 hr. The white solid which precipitated was collected by filtration and yielded 6.3 g of N-(4-chlorophenyl)thiourea, M.P. 147-148° C.

후처리

  1. customThe white solid which precipitated
  2. filtrationwas collected by filtration

출처 및 근거

ORD 기록
ord-3d7718d143754524908a18bdbe2da2b7
출처 데이터셋
uspto-grants-1999_12
특허 번호
US05998399

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