Morpholine → 3-Amino-3-morpholinoacrylonitrile

HRID 610040노트

반응식

HRID 610040 반응식
[C:1]([CH2:3][C:4](=[NH:8])OCC)#[N:2].[NH:9]1[CH2:14][CH2:13][O:12][CH2:11][CH2:10]1>C(O)C>[NH2:8][C:4]([N:9]1[CH2:14][CH2:13][O:12][CH2:11][CH2:10]1)=[CH:3][C:1]#[N:2]

참가 물질

4

반응물 2

HCID 8083MorpholineHCID 256188Ethyl 2-cyanoethanecarboximidate

생성물 1

HCID 27636313-Amino-3-morpholinoacrylonitrile

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

In anhydrous ethanol (10 ml) was dissolved ethyl 2-cyanoacetimidate (1.0 g), followed by addition of morpholine (0.78 g). The mixture was stirred at room temperature for 4 hours, and the separated crystals were collected by filtration. This crystal crop was used as it was in the next reaction.

후처리

  1. filtrationthe separated crystals were collected by filtration
  2. customwas in the next reaction

출처 및 근거

ORD 기록
ord-007f37c576bd446793605b8aa1a181ca
출처 데이터셋
uspto-grants-1999_12
특허 번호
US05998459

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