Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Aminobenzanilide → 5-Benzoyl-1-ethyl-2-oxo-2,3-dihydro-1H-indole-3-carboxylic acid (3-phenylcarbamoyl-phenyl)-amide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Aminobenzanilide | HCID 84347 | — |
| 반응물 | Ethyl 1-ethyl-5-benzoyloxindole-3-carboxylate | HCID 20189466 | — |
| 생성물 | 5-Benzoyl-1-ethyl-2-oxo-2,3-dihydro-1H-indole-3-carboxylic acid (3-phenylcarbamoyl-phenyl)-amide | HCID 54572825 | — |
반응 단계
Prepared as in Example 1, Step A, from 5-benzoyl-1-ethyl-2-oxo-2,3-dihydro-1H-indole-3-carboxylic acid ethyl ester (U.S. Pat. No. 4,686,224) and 3-amino-N-phenyl-benzamide. Purified by trituration in ethyl acetate/hexanes. mp 129-135° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05998463 |
| 출처 데이터셋 | uspto-grants-1999_12 |
| ORD ID | ord-06bff11b701640128bcbb32f0cef2f6f |
| 출처 메모 | uspto-grants-1999_12 |