반응식
CO[C:3]([CH:5]1[C:13]2[C:8](=[CH:9][CH:10]=[C:11]([C:14]3([CH3:19])[O:18]CCO3)[CH:12]=2)[N:7]([CH3:20])[C:6]1=[O:21])=[O:4].[NH2:22][C:23]1[CH:24]=[C:25]([CH:35]=[CH:36][CH:37]=1)[C:26]([NH:28][C:29]1[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1)=[O:27]>>[C:29]1([NH:28][C:26]([C:25]2[CH:24]=[C:23]([NH:22][C:3]([CH:5]3[C:13]4[C:8](=[CH:9][CH:10]=[C:11]([C:14](=[O:18])[CH3:19])[CH:12]=4)[N:7]([CH3:20])[C:6]3=[O:21])=[O:4])[CH:37]=[CH:36][CH:35]=2)=[O:27])[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1참가 물질
3
실험 절차
Prepared as in Example 1 from 1-methyl-5-(2-methyl-[1,3]dioxolan-2-yl)-2-oxo-2,3-dihydro-1H-indole-3-carboxylic acid methyl ester and 3-amino-N-phenyl-benzamide. Purified by trituration in hexanes/ethyl acetate. mp 178-179° C.
후처리
- customPurified by trituration in hexanes/ethyl acetate
출처 및 근거
- ORD 기록
- ord-aff1379f03f94e368b3e778389e43c2f
- 출처 데이터셋
- uspto-grants-1999_12
- 특허 번호
- US05998463
연결된 노트
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