Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Nitrobenzanilide → 3-Aminobenzanilide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Nitrobenzanilide | HCID 347755 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3-Aminobenzanilide | HCID 84347 | 90.8% |
반응 단계
10% Palladium on carbon (2.0 g) was added to a solution of 3-nitro-N-phenyl-benzamide (20 g, 83 mmol) in ethanol (225 mL) and the mixture was hydrogenated at 45 psi for 2 hours. The mixture was filtered through diatomaceous earth and concentrated to give a colorless solid (mp 118-120° C., 16 g, 90%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05998463 |
| 출처 데이터셋 | uspto-grants-1999_12 |
| ORD ID | ord-0de9ee7ba0624e6f89c88e7033107b63 |
| 출처 메모 | uspto-grants-1999_12 |