Phenylhydrazine → 1-(3-Bromophenyl)-3-methyl-1H-pyrazole

반응식

[Br:1][C:2]1[CH:3]=[C:4]([NH:8][NH2:9])[CH:5]=[CH:6][CH:7]=1.[C:10]1(NN)[CH:15]=CC=[CH:12][CH:11]=1>>[Br:1][C:2]1[CH:3]=[C:4]([N:8]2[CH:15]=[CH:10][C:11]([CH3:12])=[N:9]2)[CH:5]=[CH:6][CH:7]=1

참가 물질

반응물 2

HCID 7516Phenylhydrazine

HCID 33758(3-Bromophenyl)hydrazine

생성물 1

HCID 179399391-(3-Bromophenyl)-3-methyl-1H-pyrazole

실험 절차

This compound was prepared by the same methodology described for EXAMPLE 1 with 3-bromophenyl hydrazine · HCl substituted for phenyl hydrazine. There was obtained 1-(3-bromophenyl)-3-methyl-1H-pyrazole-5-[(2'-aminosulfonyl-[1,1']-biphen-4-yl)carboxyamide; HRMS(M+H)+ calc. 511.043949; found: 511.043295.

후처리

customThis compound was prepared by the same methodology

출처 및 근거

ORD 기록: ord-8f514d05ff514f33a4e81e55adc9a986
출처 데이터셋: uspto-grants-1999_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05998424

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