Phenylhydrazine → 1-(3,4-dichloro-phenyl)-3-methyl-1H-pyrazole

반응식

[Cl:1][C:2]1[CH:3]=[C:4]([NH:9][NH2:10])[CH:5]=[CH:6][C:7]=1[Cl:8].[C:11]1(NN)[CH:16]=CC=[CH:13][CH:12]=1>>[Cl:1][C:2]1[CH:3]=[C:4]([N:9]2[CH:16]=[CH:11][C:12]([CH3:13])=[N:10]2)[CH:5]=[CH:6][C:7]=1[Cl:8]

참가 물질

반응물 2

HCID 7516Phenylhydrazine

HCID 83161(3,4-Dichlorophenyl)hydrazine

생성물 1

HCID 234450371-(3,4-dichloro-phenyl)-3-methyl-1H-pyrazole

실험 절차

This compound was prepared by the same methodology described for EXAMPLE 1 with 3,4-dichlorophenyl hydrazine · HCl substituted for phenyl hydrazine. There was obtained the title compound; HRMS (M+H)+ : calc. 501.055493; found 501.053920.

후처리

customThis compound was prepared by the same methodology

출처 및 근거

ORD 기록: ord-fc73b4f2b2da4eda9ac1a0a90750ec21
출처 데이터셋: uspto-grants-1999_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05998424

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