Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetate → HCID 66870991, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetate | HCID 175 | — |
| 반응물 | Terephthalic Acid | HCID 7489 | — |
| 반응물 | Formic acid, copper salt | HCID 44152240 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 66870991 | HCID 66870991 | 42.4% |
반응 단계
0.70 g of terephthalic acid was dissolved under heating in a mixture solvent of 400 cm3 of methanol and 20 cm3 of acetate. After this solution was cooled to the normal temperature, into this solution, a further solution in which 0.95 g of formic acid copper was dissolved in 50 cm3 of methanol was dripped and then this was kept still for a few days. Thereafter, the precipitation product was suction-filtered and dried for 110° C./4 hours, whereby 0.41 g of terephthalic acid copper was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05998647 |
| 출처 데이터셋 | uspto-grants-1999_12 |
| ORD ID | ord-540d390b47ce4090addbea88f06ffda2 |
| 출처 메모 | uspto-grants-1999_12 |