Water → HCID 19600279, 화합물
반응식
CS(O[CH2:6][CH2:7][C:8]1[CH:12]=[CH:11][O:10][CH:9]=1)(=O)=O.[C:13]1(=[O:23])[NH:17][C:16](=[O:18])[C:15]2=[CH:19][CH:20]=[CH:21][CH:22]=[C:14]12.[K].O>CN(C)C=O>[O:10]1[CH:11]=[CH:12][C:8]([CH2:7][CH2:6][N:17]2[C:16](=[O:18])[C:15]3=[CH:19][CH:20]=[CH:21][CH:22]=[C:14]3[C:13]2=[O:23])=[CH:9]1참가 물질
5
반응 조건
- 온도
- 100 °C
실험 절차
To a solution of the 2-(3-furyl)ethyl methanesulfonate in 500 ml of N,N-dimethylformamide, 14.2 g (76.8 mmol) of potassium phthalimide was added, followed by overnight stirring at 100° C. After cooling to room temperature, the reaction mixture was added to water while being stirred vigorously. The resulting precipitate was filtered, washed with water and dried to yield N-[2-(3-furyl)ethyl]phthalimide.
후처리
- temperatureAfter cooling to room temperature
- stirringwhile being stirred vigorously
- filtrationThe resulting precipitate was filtered
- washwashed with water
- customdried
출처 및 근거
- ORD 기록
- ord-ee6a041d586442d5b95af9b36bd631a6
- 출처 데이터셋
- uspto-grants-1999_12
- 특허 번호
- US05998433
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