Thionyl Chloride → 2-Methoxy-6-methylbenzoyl chloride

반응식

[CH3:1][O:2][C:3]1[CH:11]=[CH:10][CH:9]=[C:8]([CH3:12])[C:4]=1[C:5](O)=[O:6].S(Cl)([Cl:15])=O>>[CH3:1][O:2][C:3]1[CH:11]=[CH:10][CH:9]=[C:8]([CH3:12])[C:4]=1[C:5]([Cl:15])=[O:6]

참가 물질

반응물 2

HCID 24386Thionyl Chloride

HCID 2731702-Methoxy-6-methylbenzoic acid

생성물 1

HCID 128926752-Methoxy-6-methylbenzoyl chloride

실험 절차

A mixture of 1A (1.7 g, 10.2 mmol) and thionyl chloride (2 ml) is heated under reflux for 1 hour. The mixture is concentrated and the resulting benzoylchloride is used without further purification.

후처리

temperatureis heated
temperatureunder reflux for 1 hour
concentrationThe mixture is concentrated
customthe resulting benzoylchloride is used without further purification

출처 및 근거

ORD 기록: ord-450ca4c394d9487ebfe0cf542fbc9cb8
출처 데이터셋: uspto-grants-1999_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06001883

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