Benzenemethanamine, 3,4-dichloro- → 4-(3,4-Dichlorophenylmethylamino)-6,7-diethoxy-3-quinolinecarbonitrile

HRID 612025

반응식

HRID 612025 반응식
Cl[C:2]1[C:11]2[C:6](=[CH:7][C:8]([O:15][CH2:16][CH3:17])=[C:9]([O:12][CH2:13][CH3:14])[CH:10]=2)[N:5]=[CH:4][C:3]=1[C:18]#[N:19].[Cl:20][C:21]1[CH:22]=[C:23]([CH:26]=[CH:27][C:28]=1[Cl:29])[CH2:24][NH2:25]>>[Cl:20][C:21]1[CH:22]=[C:23]([CH2:24][NH:25][C:2]2[C:11]3[C:6](=[CH:7][C:8]([O:15][CH2:16][CH3:17])=[C:9]([O:12][CH2:13][CH3:14])[CH:10]=3)[N:5]=[CH:4][C:3]=2[C:18]#[N:19])[CH:26]=[CH:27][C:28]=1[Cl:29]

참가 물질

3

반응물 2

HCID 1608Benzenemethanamine, 3,4-dichloro-HCID 107788724-Chloro-6,7-diethoxyquinoline-3-carbonitrile

생성물 1

HCID 101366404-(3,4-Dichlorophenylmethylamino)-6,7-diethoxy-3-quinolinecarbonitrile

실험 절차

In the manner of Example 61 reaction of 4-chloro-6,7-diethoxy-3-quinolinecarbonitrile with 3,4-dichlorobenzylamine gave the tide compound as a tan solid, mp 163-165° C.

출처 및 근거

ORD 기록
ord-ae6c997a3c4b40f696dc41a86af80cd2
출처 데이터셋
uspto-grants-1999_12
특허 번호
US06002008

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